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How is peptide purity tested?

The purity number on a certificate of analysis comes from real instruments running real tests. The two that matter most are HPLC and mass spectrometry. Here is what each one does.

5 min read Reviewed for accuracy Research Use Only
The short answer

Peptide purity is tested primarily by HPLC, which measures the target peptide as a percentage of the sample, and mass spectrometry, which confirms identity by molecular weight. HPLC answers how pure; mass spec answers is it the right molecule.

HPLC: measuring purity

High-performance liquid chromatography pushes the sample through a column that separates it into its components. The target peptide appears as the main peak, and its share of the total is reported as the purity percentage. A single tall, dominant peak indicates high purity.

retention time signal target peptide 99.4%+
On an HPLC chromatogram, a single tall, dominant peak indicates a high-purity peptide.

Mass spectrometry: confirming identity

Mass spectrometry measures the molecular weight of the peptide. Because each sequence has a known expected weight, a match confirms the material is the correct molecule, not a similar impurity.

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Why both are needed

Purity without identity is not enough, and vice versa. A peptide could be highly pure but the wrong molecule, or the right molecule but impure. Running both tests and reporting them on a certificate of analysis is what confirms a peptide is both pure and correct.

Key takeaways

  • HPLC separates the sample and reports purity as an area percentage.
  • A single dominant HPLC peak indicates high purity.
  • Mass spectrometry confirms identity by molecular weight.
  • Together they verify both purity and identity on the COA.

A note on research use

The peptides supplied by Axis Peptide Labs are reference compounds for laboratory and research use only. They are intended for qualified researchers working in academic, institutional, and analytical settings. They are not drugs, foods, cosmetics, or medical products, and they are not intended for human or veterinary consumption. Documented identity and documented purity are what matter most when sourcing a compound, both of which are published on the Axis certificates of analysis page.

Every compound is tested. Every certificate is public.

Browse the Axis Peptide Labs catalog of third-party tested research peptides, each with a published certificate of analysis.

Axis Peptide Labs supplies reference compounds for laboratory, academic, and institutional research only. All products are for research and identification purposes only. They are not for human or veterinary use, and are not a food, cosmetic, drug, or medical product. This article is educational and does not constitute medical, health, or usage advice.

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